5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

Base Information

Chemical Name:5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole
CAS No.:1338068-90-8
Molecular Formula:C₃₆H₃₁BN₂O₂
Molecular Weight:534.465
Hs Code.:

Synonyms:5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

There total 6 articles about 5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1338068-89-5
C₃₀H₁₉IN₂

: 73183-34-3
bis(pinacol)diborane

: 1338068-90-8
5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; at 90 ℃; for 6h; Inert atmosphere;

Reference yield: 77.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 2-bromo-5,11-diphenyl-5,11-dihydroindolo[3,2-b]carbazole

: 1338068-90-8
5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:: 2-bromo-5,11-diphenyl-5,11-dihydroindolo[3,2-b]carbazole; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 ℃; for 6h;

Reference yield: 58.0%

: 1338068-90-8
5,11-diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:: With palladium (II) [1,1'-bis(diphenylphosphanyl)ferrocene] dichloride; anhydrous potassium acetate; In 1,4-dioxane; for 3.5h; Reflux;