(S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

Base Information

Chemical Name:(S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol
CAS No.:132316-98-4
Molecular Formula:C₂₆H₃₉NO₄Si
Molecular Weight:457.685
Hs Code.:

(S)-2-<N-benzyl-N-(benzyloxycarbonyl)amino>-5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

Synonyms:(S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

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Chemical Property of (S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

Chemical Property:

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Technology Process of (S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

There total 5 articles about (S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 132316-97-3
(S)-2--1,5-pentanediol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 132316-98-4
(S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

Guidance literature:: With pyridine;
DOI:10.1016/S0040-4039(00)97867-5

Reference yield:

: 77539-18-5,73914-82-6
(S)-(+)-2-benzylamino glutaric acid

: 132316-98-4
(S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / NaHCO₃ / H₂O / 3 h / Ambient temperature

2: 70 percent / BH₃*THF / tetrahydrofuran / 18 h / Ambient temperature

3: 88 percent / pyridine, DMAP / CH₂Cl₂ / 18 h / Ambient temperature

With pyridine; dmap; borane-THF; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo00040a045

Reference yield:

: 132316-96-2
(S)-N-benzyl-N-(benzyloxycarbonyl)glutamic acid

: 132316-98-4
(S)-2--5-<(tert-butyldimethylsilyl)oxy>pentan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / BH₃*THF / tetrahydrofuran / 18 h / Ambient temperature

2: 88 percent / pyridine, DMAP / CH₂Cl₂ / 18 h / Ambient temperature

With pyridine; dmap; borane-THF; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00040a045