Technology Process of 5-Allyloxy-2,4-diisopropoxyacetophenone
There total 4 articles about 5-Allyloxy-2,4-diisopropoxyacetophenone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic anhydride;
In
dichloromethane;
for 72h;
DOI:10.1039/a908367g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / phosphoryl trichloride / toluene / 2.5 h / 0 - 120 °C
2: 63 percent / MMPP / methanol / 60 h / 20 °C
3: 94 percent / K2CO3 / acetone / 48 h / Heating
4: 94 percent / TFAA / CH2Cl2 / 72 h
With
potassium carbonate; trifluoroacetic anhydride; trichlorophosphate;
In
methanol; dichloromethane; acetone; toluene;
1: Formylation / 2: Reduction / 3: Etherification / 4: Acylation;
DOI:10.1039/a908367g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 63 percent / MMPP / methanol / 60 h / 20 °C
2: 94 percent / K2CO3 / acetone / 48 h / Heating
3: 94 percent / TFAA / CH2Cl2 / 72 h
With
potassium carbonate; trifluoroacetic anhydride;
In
methanol; dichloromethane; acetone;
1: Reduction / 2: Etherification / 3: Acylation;
DOI:10.1039/a908367g
