N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

Base Information

Chemical Name:N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide
CAS No.:1094628-96-2
Molecular Formula:C₂₀H₂₁N₃O₅
Molecular Weight:383.404
Hs Code.:

Synonyms:N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

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Chemical Property of N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

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Technology Process of N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

There total 2 articles about N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1094628-91-7
1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxylic acid

: 1094628-96-2
N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

Guidance literature:: With N-methoxylamine hydrochloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.04.076

Reference yield: 85.0%

: 1094628-91-7
1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxylic acid

: 593-56-6
N-methoxylamine hydrochloride

: 1094628-96-2
N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In acetonitrile;
DOI:10.1016/j.tetlet.2008.09.098

Reference yield: 50.0%

: 1094628-96-2
N-methoxy-1-(4'-methoxyphenyl)-3-(3'',4''-dimethoxyphenyl)-1H-pyrazole-4-carboxamide

: 1094629-01-2
5,7,8-trimethoxy-2-(4'-methoxyphenyl)-2H-pyrazolo[4,3-c]quinolin-4(5H)-one

Guidance literature:: With trifluoroacetic acid; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; at -20 ℃; for 1h;
DOI:10.1016/j.tetlet.2008.09.098