Technology Process of C60H37N3O
There total 4 articles about C60H37N3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
toluene;
at 80 ℃;
for 8h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium iodide; potassium iodate; sulfuric acid / ethanol / 2 h / 75 °C
2.1: n-butyllithium / toluene; hexane; diethyl ether / 3 h / -45 - -5 °C / Inert atmosphere
2.2: -45 - 20 °C
2.3: 20 °C
3.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; water; 1,2-dimethoxyethane / 10 h / Inert atmosphere; Reflux
4.1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate / toluene / 8 h / 80 °C / Inert atmosphere
With
potassium iodate; tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); n-butyllithium; sulfuric acid; sodium carbonate; potassium iodide; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
1,2-dimethoxyethane; diethyl ether; ethanol; hexane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / toluene; hexane; diethyl ether / 3 h / -45 - -5 °C / Inert atmosphere
1.2: -45 - 20 °C
1.3: 20 °C
2.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; water; 1,2-dimethoxyethane / 10 h / Inert atmosphere; Reflux
3.1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate / toluene / 8 h / 80 °C / Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); n-butyllithium; sodium carbonate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
1,2-dimethoxyethane; diethyl ether; hexane; water; toluene;