3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

Base Information

Chemical Name:3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]
CAS No.:292605-27-7
Molecular Formula:C₂₁H₁₈N₂O₄
Molecular Weight:362.385
Hs Code.:

Synonyms:3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

Suppliers and Price of 3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

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Technology Process of 3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

There total 2 articles about 3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 108-28-1
protoanemonin

: 36288-37-6
N-hydroxy-4-methylbenzenecarboximidoyl chloride

: 292605-27-7
3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

Guidance literature:: With triethylamine; hydroquinone; In diethyl ether; at 20 ℃;
DOI:10.1039/b001481h

Reference yield: 50.0%

: 108-28-1
protoanemonin

: 36288-37-6
N-hydroxy-4-methylbenzenecarboximidoyl chloride

: anemonin

: 292605-27-7
3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

: 292605-23-3
2,5-dihydro-3'-(p-tolyl)spiroisoxazolino-[5',5]furan-2-one

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 24h;
DOI:10.1039/b001481h

Reference yield: 91.0%

: 292605-27-7
3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]

: 3,3'-Di-p-tolyl-4,5-dihydro-[5,5']biisoxazolyl

Guidance literature:: 3,3'-bis(p-tolyl)-3a,6a-dihydro-4-oxospiro[isoxazolino-5',6-isoxazolo[3,4-c]furanone]; With sodium hydroxide; In ethanol; water; at 20 ℃; for 2h;

With sulfuric acid; In ethanol; water; for 24h; Further stages.; Heating;
DOI:10.1039/b001481h