1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

Base Information

Chemical Name:1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene
CAS No.:1607796-21-3
Molecular Formula:C₁₅H₁₃F₇O₂
Molecular Weight:358.256
Hs Code.:

Synonyms:1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

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Technology Process of 1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

There total 1 articles about 1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 906623-17-4
4-bromo-1-(methoxymethoxy)-3,5-dimethylbenzene

: 559-40-0
octaperfluorocyclopentene

: 1607796-21-3
1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

Guidance literature:: 4-bromo-1-(methoxymethoxy)-3,5-dimethylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

octaperfluorocyclopentene; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere;
DOI:10.1246/bcsj.20130252

Reference yield: 74.0%

: 1607796-21-3
1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

: 348639-00-9
3-bromo-2-methyl-5-thiophenecarboxyaldehyde 2,2-dimethylpropan-1,3-diyl acetal

: 1607796-24-6
1-[5-(5,5-dimethyl-1,3-dioxacyclohexane-2-yl)-2-methyl-3-thienyl]-2-(4-methoxymethoxy-2,6-dimethylphenyl)-3,3,4,4,5,5-hexafluorocyclopentene

Guidance literature:: 3-bromo-2-methyl-5-thiophenecarboxyaldehyde 2,2-dimethylpropan-1,3-diyl acetal; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene; In tetrahydrofuran; hexane; at -78 - 30 ℃; for 12h;
DOI:10.1246/bcsj.20130252

Reference yield: 54.0%

: 31819-37-1
3-bromo-2,5-dimethylthiophene

: 1607796-21-3
1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene

: 1607796-23-5
1-(4-methoxymethoxy-2,6-dimethylphenyl)-2-(2,5-dimethyl-3-thienyl)-3,3,4,4,5,5-hexafluorocyclopentene

Guidance literature:: 3-bromo-2,5-dimethylthiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

1-(4-methoxymethoxy-2,6-dimethylphenyl)-2,3,3,4,4,5,5-heptafluorocyclopentene; In tetrahydrofuran; hexane; at -78 ℃; for 3.5h; Inert atmosphere;
DOI:10.1246/bcsj.20130252