(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

Base Information

Chemical Name:(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal
CAS No.:170707-52-5
Molecular Formula:C₁₆H₂₃NO₇
Molecular Weight:341.361
Hs Code.:

Synonyms:(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

Suppliers and Price of (2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

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Technology Process of (2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

There total 8 articles about (2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 170707-51-4
(2R,3S,5S,6R)-6-(2,5-Dimethoxy-3-nitro-phenyl)-3,6-dimethoxy-5-methyl-hexane-1,2-diol

: 170707-52-5
(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

Guidance literature:: With sodium periodate; sodium hydrogencarbonate; In acetone; for 1.66667h; Ambient temperature;
DOI:10.1021/ja974318b

Reference yield:

: 170707-50-3
(2R,3S,5S,6R)-2-Benzyloxy-6-(2,5-dimethoxy-3-nitro-phenyl)-3,6-dimethoxy-5-methyl-hexan-1-ol

: 170707-52-5
(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

Guidance literature:: (2R,3S,5S,6R)-2-Benzyloxy-6-(2,5-dimethoxy-3-nitro-phenyl)-3,6-dimethoxy-5-methyl-hexan-1-ol; With boron trichloride - methyl sulfide complex;

With sodium periodate;
DOI:10.1021/ol036092p

Reference yield:

: 170901-52-7
(2R,3S,5S,6R)-2-Benzyloxy-6-(2,5-dimethoxy-3-nitro-phenyl)-6-methoxy-5-methyl-hexane-1,3-diol

: 170707-52-5
(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: 98 percent / TBAF

2.1: BCl₃*SMe₂

2.2: NaIO₄

With boron trichloride - methyl sulfide complex; tetrabutyl ammonium fluoride;
DOI:10.1021/ol036092p