3-Decenoic acid, 10-(2,5-dimethoxy-3-nitrophenyl)-6,7,10-trimethoxy-5,9-dimethyl-, methyl ester, (3E,5S,6R,7S,9S,10R)-

Base Information

Chemical Name:3-Decenoic acid, 10-(2,5-dimethoxy-3-nitrophenyl)-6,7,10-trimethoxy-5,9-dimethyl-, methyl ester, (3E,5S,6R,7S,9S,10R)-
CAS No.:170707-53-6
Molecular Formula:C24H37NO9
Molecular Weight:483.559
Hs Code.:
Mol file:170707-53-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Decenoic acid, 10-(2,5-dimethoxy-3-nitrophenyl)-6,7,10-trimethoxy-5,9-dimethyl-, methyl ester, (3E,5S,6R,7S,9S,10R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Decenoic acid, 10-(2,5-dimethoxy-3-nitrophenyl)-6,7,10-trimethoxy-5,9-dimethyl-, methyl ester, (3E,5S,6R,7S,9S,10R)-

There total 6 articles about 3-Decenoic acid, 10-(2,5-dimethoxy-3-nitrophenyl)-6,7,10-trimethoxy-5,9-dimethyl-, methyl ester, (3E,5S,6R,7S,9S,10R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1825-61-2
Trimethylmethoxysilane

: 136314-66-4
methyl (3S,4E)-3-(dimethylphenylsilyl)-4-hexenoate

: 170707-52-5
(2S,4S,5R)-5-(2,5-dimethoxy-3-nitrophenyl)-2,5-dimethoxy-4-methylpentanal

: 170707-53-6
(E)-(5S,6R,7S,9S,10R)-10-(2,5-Dimethoxy-3-nitro-phenyl)-6,7,10-trimethoxy-5,9-dimethyl-dec-3-enoic acid methyl ester

: (E)-(5S,6S,7S,9S,10R)-10-(2,5-Dimethoxy-3-nitro-phenyl)-6,7,10-trimethoxy-5,9-dimethyl-dec-3-enoic acid methyl ester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -50 ℃; for 42h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja974318b

Reference yield:

: 170707-49-0
[(2R,3S,5S,6R)-2-Benzyloxy-6-(2,5-dimethoxy-3-nitro-phenyl)-3,6-dimethoxy-5-methyl-hexyloxy]-tert-butyl-dimethyl-silane

: 170707-53-6
(E)-(5S,6R,7S,9S,10R)-10-(2,5-Dimethoxy-3-nitro-phenyl)-6,7,10-trimethoxy-5,9-dimethyl-dec-3-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 98 percent / TBAF

2.1: BCl₃*SMe₂

2.2: NaIO₄

3.1: TMSOTf

With trimethylsilyl trifluoromethanesulfonate; boron trichloride - methyl sulfide complex; tetrabutyl ammonium fluoride;
DOI:10.1021/ol036092p

Reference yield:

: 170901-52-7
(2R,3S,5S,6R)-2-Benzyloxy-6-(2,5-dimethoxy-3-nitro-phenyl)-6-methoxy-5-methyl-hexane-1,3-diol

: 170707-53-6
(E)-(5S,6R,7S,9S,10R)-10-(2,5-Dimethoxy-3-nitro-phenyl)-6,7,10-trimethoxy-5,9-dimethyl-dec-3-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 98 percent / TBAF

2.1: BCl₃*SMe₂

2.2: NaIO₄

3.1: TMSOTf

With trimethylsilyl trifluoromethanesulfonate; boron trichloride - methyl sulfide complex; tetrabutyl ammonium fluoride;
DOI:10.1021/ol036092p