Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-ba-,6a-ba-)]- (9CI)

Base Information

Chemical Name:Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-ba-,6a-ba-)]- (9CI)
CAS No.:156366-59-5
Molecular Formula:C₉H₁₇NO
Molecular Weight:155.24
Hs Code.:
Mol file:156366-59-5.mol

Synonyms:Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-b閠a-,6a-b閠a-)]- (9CI);Cyclopenta[b]pyrrole-2-methanol,octahydro-1-methyl-,[2R-(2-alpha-,3a-bta-,6a-bta-)]-(9CI)

Suppliers and Price of Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-ba-,6a-ba-)]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-ba-,6a-ba-)]- (9CI)

Chemical Property:

Boiling Point:47 °C (0.008 mmHg)
PSA：23.47000
LogP:0.78940

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-ba-,6a-ba-)]- (9CI)

There total 2 articles about Cyclopenta[b]pyrrole-2-methanol, octahydro-1-methyl-, [2R-(2-alpha-,3a-ba-,6a-ba-)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 155682-95-4
(1R,3R,5R)-3-(hydroxymethyl)-2-azabicyclo-<3.3.0>-octane

: 156366-59-5,193606-60-9
(all-R)-3-(Hydroxymethyl)-2-methyl-2-azabicyclo<3.3.0>octan

Guidance literature:: In formic acid; water; for 8h; Heating;

Reference yield:

: 129101-19-5
(all-R)-2-Azabicyclo[3.3.0]octan-3-oic acid benzyl ester p-toluenesulfonate

: 156366-59-5,193606-60-9
(all-R)-3-(Hydroxymethyl)-2-methyl-2-azabicyclo<3.3.0>octan

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LiAlH₄, 2.) KOH / 1.) THF, reflux, 3 h, 2.) THF, water, reflux, 45 min

2: 86 percent / formic acid; H₂O / 8 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; In formic acid; water;