Cyclopenta[b]pyrrole-1(2H)-ethanol, hexahydro-, (3aR,6aR)- (9CI)

Base Information

• Chemical Name: Cyclopenta[b]pyrrole-1(2H)-ethanol, hexahydro-, (3aR,6aR)- (9CI)
• CAS No.: 156366-41-5
• Molecular Formula: C₉H₁₇NO
• Molecular Weight: 155.24
• Mol file: 156366-41-5.mol

Synonyms:Cyclopenta[b]pyrrole-1(2H)-ethanol,hexahydro-, (3aR-cis)-

Chemical Property of Cyclopenta[b]pyrrole-1(2H)-ethanol, hexahydro-, (3aR,6aR)- (9CI)

Chemical Property:

• PSA: 23.47000
• LogP: 0.79100

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Cyclopenta[b]pyrrole-1(2H)-ethanol, hexahydro-, (3aR,6aR)- (9CI)

There total 5 articles about Cyclopenta[b]pyrrole-1(2H)-ethanol, hexahydro-, (3aR,6aR)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Methyl (1'R,5'R)-(-)-2-(2'-azabicyclo[3.3.0]octan-2'-yl)acetate (250370-86-6) → (1R,5R)-2-(2'-Hydroxyethyl)-2-azabicyclo<3.3.0>octan (156366-41-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Heating;

DOI:10.1039/a902362c

Reference yield: 81.0%

oxirane (75-21-8,99932-75-9) + (3aR,6aR)-octahydrocyclopentapyrrole (156473-27-7) → (1R,5R)-2-(2'-Hydroxyethyl)-2-azabicyclo<3.3.0>octan (156366-41-5)

Guidance literature:

In methanol; for 2h; Ambient temperature;

Reference yield: 79.0%

(1R,5R)-2-Azabicyclo<3.3.0>octan-2-essigsaeure-ethylester (156366-40-4) → (1R,5R)-2-(2'-Hydroxyethyl)-2-azabicyclo<3.3.0>octan (156366-41-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 6h; Heating;

upstream raw materials:

oxirane

(3aR,6aR)-octahydrocyclopentapyrrole

(1R,5R)-2-Azabicyclo<3.3.0>octan-2-essigsaeure-ethylester

Methyl (1'R,5'R)-(-)-2-(2'-azabicyclo[3.3.0]octan-2'-yl)acetate

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