αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane

Base Information

• Chemical Name: αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane
• CAS No.: 101980-97-6
• Molecular Formula: C₂₉H₁₇Cl₁₄NO₅
• Molecular Weight: 955.8

Synonyms:αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane

Chemical Property of αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane

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Technology Process of αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane

There total 7 articles about αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

6,6'-((4-(bromomethyl)-2,3,5,6-tetrachlorophenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene) (101998-20-3) + 2-acetylaminomalonic acid diethyl ester (1068-90-2) → αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane (101980-97-6)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; for 48h; Heating;

DOI:10.1021/jo00363a013

Reference yield: 76.0%

2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene (101980-93-2) + 2-acetylaminomalonic acid diethyl ester (1068-90-2) → αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane (101980-97-6)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; for 48h; Heating;

DOI:10.1021/jo00363a013

Reference yield: 52.0%

4-(bromomethyl)tetradecachlorotriphenylmethyl radical (81221-80-9) + 2-acetylaminomalonic acid diethyl ester (1068-90-2) → αH-4-(2-acetamido-2,2-bis(ethoxycarbonyl)ethyl)tetradecachlorotriphenylmethane (101980-97-6)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; for 24h; Heating;

DOI:10.1021/jo00363a013

upstream raw materials:

4-(bromomethyl)tetradecachlorotriphenylmethyl radical

2-acetylaminomalonic acid diethyl ester

6,6'-((4-(bromomethyl)-2,3,5,6-tetrachlorophenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene)

2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

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