2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

Base Information

Chemical Name:2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene
CAS No.:101980-93-2
Molecular Formula:C₂₇H₁₀Cl₁₄O₃S
Molecular Weight:910.783
Hs Code.:

Synonyms:2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

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Chemical Property of 2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

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Technology Process of 2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

There total 5 articles about 2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 16836-95-6
silver(I) 4-methylbenzenesulfonate

: 101998-20-3
6,6'-((4-(bromomethyl)-2,3,5,6-tetrachlorophenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene)

: 101980-93-2
2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

Guidance literature:: In 1,4-dioxane; acetonitrile; at 70 ℃; for 24h;
DOI:10.1021/jo00363a013

Reference yield: 87.0%

: 101980-98-7
2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-hydroxytoluene

: 98-59-9
p-toluenesulfonyl chloride

: 101980-93-2
2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 35h; Ambient temperature;
DOI:10.1021/jo00363a013

Reference yield:

: 79839-38-6
6,6’-((2,3,5,6-tetrachloro-4-methylphenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene)

: 101980-93-2
2,3,5,6-tetrachloro-4-(bis(pentachlorophenyl)methyl)-α-(tosyloxy)toluene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Br₂ / CCl₄ / 5 h / Irradiation

2: 82 percent / acetic acid / 72 h / Heating

3: 85 percent / aq. concd HCl / dioxane / 21 h / Heating

4: 87 percent / aq. NaOH / dioxane / 35 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; bromine; In 1,4-dioxane; tetrachloromethane; acetic acid;
DOI:10.1021/jo00363a013