Cu(C₇₀H₆₆N₈O₁₈)Cu((CH₃)3CC₆H₃(O)(CHN))2

Base Information

• Chemical Name: Cu(C₇₀H₆₆N₈O₁₈)Cu((CH₃)3CC₆H₃(O)(CHN))2
• CAS No.: 862158-85-8
• Molecular Formula: C₉₂H₉₂Cu₂N₁₀O₂₀
• Molecular Weight: 1784.89
• Mol file: 862158-85-8.mol

Synonyms:Cu(C₇₀H₆₆N₈O₁₈)Cu((CH₃)3CC₆H₃(O)(CHN))2

Chemical Property of Cu(C₇₀H₆₆N₈O₁₈)Cu((CH₃)3CC₆H₃(O)(CHN))2

Chemical Property:

Purity/Quality:

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Technology Process of Cu(C₇₀H₆₆N₈O₁₈)Cu((CH₃)3CC₆H₃(O)(CHN))2

There total 1 articles about Cu(C₇₀H₆₆N₈O₁₈)Cu((CH₃)3CC₆H₃(O)(CHN))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

CuN8C16(C6H2(OCH3)3)6N2Se (716319-52-7) + 2-hydroxy-5-t-butylbenzaldehyde (2725-53-3) + copper dichloride → Cu(C70H66N8O18)Cu((CH3)3CC6H3(O)(CHN))2 (862158-85-8)

Guidance literature:

With H₂S; triethylamine; In pyridine; methanol; chloroform; dry N2, Cu-compd. and benzaldehyde-compd. put into a three-neck round-bottom, anhydrous pyridine added, H2S bubbled for 5 min, solv. evapd. in vac., chromy. (4% CH3OH in CHCl3), dissolved in CHCl3 and CH3OH, 1:1, CuCl2 and Et3N added, refluxed for 2 h; column chromy. (silica gel, 4% CH3OH in CHCl3);

DOI:10.1021/ja0438112

upstream raw materials:

CuN₈C₁₆(C₆H₂(OCH₃)3)6N₂Se

2-hydroxy-5-t-butylbenzaldehyde