C₂₅H₃₃N₅O₉

Base Information

Chemical Name:C₂₅H₃₃N₅O₉
CAS No.:1430098-23-9
Molecular Formula:C₂₅H₃₃N₅O₉
Molecular Weight:547.565
Hs Code.:

C<sub>25</sub>H<sub>33</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₂₅H₃₃N₅O₉

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Chemical Property of C₂₅H₃₃N₅O₉

Chemical Property:

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Technology Process of C₂₅H₃₃N₅O₉

There total 15 articles about C₂₅H₃₃N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₃₉N₅O₉

: 1430098-23-9
C₂₅H₃₃N₅O₉

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.12.111

Reference yield:

: 634-97-9
pyrrole-2-carboxyl acid

: 1430098-23-9
C₂₅H₃₃N₅O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 4 h / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 760.05 Torr / Inert atmosphere

4.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

8.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / Inert atmosphere

With oxalyl dichloride; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2012.12.111

Reference yield:

: 5427-82-7
1H-pyrrole-2-carbonyl chloride

: 1430098-23-9
C₂₅H₃₃N₅O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 760.05 Torr / Inert atmosphere

3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2012.12.111