4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride

Base Information

• Chemical Name: 4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride
• CAS No.: 675137-47-0
• Molecular Formula: C₁₈H₂₄ClN₃O₄S
• Molecular Weight: 413.925

Synonyms:4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride

Chemical Property of 4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride

Chemical Property:

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Technology Process of 4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride

There total 1 articles about 4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-{[N-boc(N-1H-imidazol-2-ylmethyl)amino]methyl} benzyl alcohol (675137-09-4) + methanesulfonyl chloride (124-63-0) → 4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride (675137-47-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride (675137-47-0) + 4-(dipropylamino)-1-butanol (70289-17-7) → [4-(4-{[N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyloxyl) butyl]dipropylamine

Guidance literature:

With potassium hydrogencarbonate; In dichloromethane; at 20 ℃; for 144h;

Reference yield:

4-{N-boc(N-1-methanesulfonyl-1H-imidazol-2-ylmethyl)aminomethyl}benzylchloride (675137-47-0) + 4-(2-dipropylamino-ethyl)-phenol (96886-46-3) → {2-[4-(4-{[N-boc(N-1-methane sulfonyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyloxy) phenyl]ethyl}dipropylamine

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 72h;

upstream raw materials:

4-{[N-boc(N-1H-imidazol-2-ylmethyl)amino]methyl} benzyl alcohol

methanesulfonyl chloride

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