[Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

Base Information

Chemical Name:[Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)
CAS No.:127540-58-3
Molecular Formula:C₃₆H₃₂Co₂O₄P₂Si
Molecular Weight:736.667
Hs Code.:

[Co<sub>2</sub>(CO)<sub>4</sub>(μ-bis(diphenylphosphino)methane)(μ<sub>2</sub>-η<sup>2</sup>-SiMe<sub>3</sub>C<sub>2</sub>)](CΞCH)

Synonyms:[Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

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Technology Process of [Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

There total 5 articles about [Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 127570-42-7
Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

: 429-41-4
tetrabutyl ammonium fluoride

: 127540-58-3
[Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

Guidance literature:: In tetrahydrofuran; methanol; refluxing (THF/MeOH 10:1, 12 h);
DOI:10.1021/ja00168a056

Reference yield: 80.0%

: 127570-42-7
Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

: 127540-58-3
[Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

Guidance literature:: With Bu₄NF; In tetrahydrofuran; methanol; (N2); stirring (1-2 h); solvent removal, dissoln. (MeOH), crystn. on standing;
DOI:10.1039/dt9960001551

Reference yield:

: 2071-20-7
bis-diphenylphosphinomethane

: 127540-58-3
[Co₂(CO)₄(μ-bis(diphenylphosphino)methane)(μ₂-η²-SiMe₃C₂)](CΞCH)

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: tetrahydrofuran; methanol

In tetrahydrofuran; methanol; benzene;
DOI:10.1021/ja00168a056