(S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

Base Information

Chemical Name:(S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane
CAS No.:953076-21-6
Molecular Formula:C₂₇H₃₂N₄O₃SSi
Molecular Weight:520.728
Hs Code.:

Synonyms:(S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

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Technology Process of (S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

There total 5 articles about (S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 953076-20-5
C₂₇H₃₂N₄OSSi

: 953076-21-6
(S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

Guidance literature:: With ammonium heptamolybdate; dihydrogen peroxide; In ethanol; at 20 ℃; for 4h;
DOI:10.1016/j.tetasy.2007.07.010

Reference yield:

: 95514-04-8
(R)-3-(tert-butyldiphenylsilyloxy)-2-methylpropan-1-ol

: 953076-21-6
(S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Ph₃P; diethyl azodicarboxylate / toluene; tetrahydrofuran / 3 h / 20 °C

2: 59 percent / (NH₄)6Mo₇O₂₄*4H₂O; aq. H₂O₂ / ethanol / 4 h / 20 °C

With ammonium heptamolybdate; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/j.tetasy.2007.07.010

Reference yield:

: 95514-03-7
(S)-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propionic acid methyl ester

: 953076-21-6
(S)-3-(1'-phenyl-1'H-tetrazole-5'-sulfanyl)-1-tert-butyldiphenylsilyloxy-2-methylpropane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / LiBH₄ / tetrahydrofuran / 6 h / 50 °C

2: 96 percent / Ph₃P; diethyl azodicarboxylate / toluene; tetrahydrofuran / 3 h / 20 °C

3: 59 percent / (NH₄)6Mo₇O₂₄*4H₂O; aq. H₂O₂ / ethanol / 4 h / 20 °C

With ammonium heptamolybdate; lithium borohydride; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/j.tetasy.2007.07.010