1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

Base Information

Chemical Name:1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene
CAS No.:1338444-62-4
Molecular Formula:C₄₀H₄₄F₆O₂
Molecular Weight:670.779
Hs Code.:

Synonyms:1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

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Technology Process of 1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

There total 3 articles about 1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-hexyloxy-2,3-difluorophenyl)cyclohexan-4-one: 1277641-40-3
1-(4-hexyloxy-2,3-difluorophenyl)cyclohexan-4-one

: 1338448-92-2
1-butoxy-4-[4-(2,3-difluorophenyl)cyclohex-1-enyl]-2,3-difluorobenzene

: 598-30-1
sec.-butyllithium

: 1338444-62-4
1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

Guidance literature:: With ammonium chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; water; ethyl acetate; toluene;

Reference yield:

: 1277641-39-0
8-(4-hexyloxy-2,3-difluorophenyl)-1,4-dioxaspiro[4.5]decane

: 1338444-62-4
1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; formic acid / toluene; water

2: toluene-4-sulfonic acid; ammonium chloride; sodium hydrogencarbonate / ethyl acetate; toluene; hexane; water; tetrahydrofuran

With formic acid; ammonium chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; water; ethyl acetate; toluene;

Reference yield:

: 196960-06-2
4-(2,3-difluorophenyl)cyclohexan-1-one

: 136239-66-2
2,3-difluorophenyl butyl ether

: 1338444-62-4
1-butoxy-4-(4-(4-(4-(2,3-difluoro-4-hexyloxyphenyl)cyclohex-1-enyl)-2,3-difluorophenyl)cyclohex-1-en yl)-2,3-difluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid; ammonium chloride; sodium hydrogencarbonate / ethyl acetate; toluene; hexane; water; tetrahydrofuran

2: toluene-4-sulfonic acid; ammonium chloride; sodium hydrogencarbonate / ethyl acetate; toluene; hexane; water; tetrahydrofuran

With ammonium chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; water; ethyl acetate; toluene;