{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester
CAS No.:206991-22-2
Molecular Formula:C₃₆H₃₃Br₄N₃O₇
Molecular Weight:939.29
Hs Code.:

{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Synonyms:{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

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Chemical Property of {2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of {2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

There total 8 articles about {2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 206991-24-4
{2-[4-(3-{3-(2-Benzyloxy-3,5-dibromo-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-3,5-dibromo-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

: 206991-22-2
{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; acetic acid; for 3h; Ambient temperature;

Reference yield:

: 134755-34-3
3,5-dibromo-4-hydroxy-β-phenethylamine

: 206991-22-2
{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / acetic acid; dimethylformamide / 6 h / 100 °C

2: 75 percent / dimethylformamide / 5 h / 110 °C

3: 85percent hydrazine hydrate / methanol / 2 h / Heating

4: 82 percent / CH₂Cl₂ / 13 h / Ambient temperature

5: 367 mg / 33percent HBr / acetic acid / 3 h / Ambient temperature

6: 52 percent / DCC, N-hydroxyphthalimide / dioxane / 2 h / Ambient temperature

7: 62 percent / H₂ / 10percent Pd/C / acetic acid; dioxane / 3 h / Ambient temperature

With N-hydroxyphthalimide; hydrogen bromide; hydrogen; hydrazine hydrate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 206991-22-2
{2-[3,5-Dibromo-4-(3-{3-(3,5-dibromo-2-hydroxy-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionylamino}-propoxy)-phenyl]-ethyl}-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / CH₂Cl₂ / 13 h / Ambient temperature

2: 367 mg / 33percent HBr / acetic acid / 3 h / Ambient temperature

3: 52 percent / DCC, N-hydroxyphthalimide / dioxane / 2 h / Ambient temperature

4: 62 percent / H₂ / 10percent Pd/C / acetic acid; dioxane / 3 h / Ambient temperature

With N-hydroxyphthalimide; hydrogen bromide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; acetic acid;