<1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester

Base Information

Chemical Name:<1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester
CAS No.:132294-27-0
Molecular Formula:C₃₂H₂₉N₅O₅
Molecular Weight:563.613
Hs Code.:

Synonyms:<1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester

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Chemical Property of <1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester

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Technology Process of <1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester

There total 10 articles about <1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 132294-26-9
<1R-(1α,2β,3β)>-3-<<(4-methylphenyl)sulfonyl>oxy>-1,2-cyclobutanedimethanol dibenzoate ester

: 19916-73-5
2-Amino-6-benzyloxypurine

: 132294-27-0
<1R-(1α,2β,3α)>-3-<2-amino-6-(phenylmethoxy)-9H-purin-9-yl>-1,2-cyclobutanedimethanol 1,2-dibenzoate ester

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 21h;
DOI:10.1021/jm00108a026

Reference yield: 40.0%

: 126261-74-3,127759-91-5,132294-18-9,132294-26-9
(1α,2β,3β)-3-<<(4-methylphenyl)sulfonyl>oxy>-1,2-cyclobutanedimethanol, dibenzoate ester

: 19916-73-5
2-Amino-6-benzyloxypurine

: 126261-75-4,127759-92-6,132294-19-0,132294-27-0
C₃₂H₂₉N₅O₅

Guidance literature:: With potassium carbonate; 18-crown-6 ether; In N,N-dimethyl-formamide; at 110 ℃; for 16h;
DOI:10.1016/S0040-4039(01)88992-9

Reference yield:

: 126261-73-2,126373-88-4,127759-90-4,127759-93-7,132294-17-8,132294-25-8
C₂₀H₂₀O₅

: 126261-75-4,127759-92-6,132294-19-0,132294-27-0
C₃₂H₂₉N₅O₅

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / pyridine / 16 h / 60 °C

2: 40 percent / K₂CO₃ / 18-crown-6 / dimethylformamide / 16 h / 110 °C

With potassium carbonate; 18-crown-6 ether; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)88992-9