(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

Base Information

Chemical Name:(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride
CAS No.:1443156-35-1
Molecular Formula:C₂₁H₂₇NO*ClH
Molecular Weight:345.912
Hs Code.:

Synonyms:(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

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Chemical Property of (2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of (2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

There total 8 articles about (2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1367878-83-8
(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine

: 1443156-35-1
(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

Guidance literature:: With hydrogenchloride; In tert-butyl methyl ether; water; acetonitrile; at 40 ℃;

Reference yield:

: 155697-42-0
(E)-3-(3-(benzyloxy)phenyl)prop-2-en-1-ol

: 1443156-35-1
(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 18 h / 20 - 40 °C / Inert atmosphere

2: bis(1,5-cyclooctadiene)diiridium(I) dichloride; tricyclohexylphosphine; sodium tetraphenyl borate / dichloromethane; acetone / 14 h / 20 °C / Inert atmosphere

3: 4-(dimethylamino)-N-((1R,2S)-2-hydroxy-2,3-dihydro-1H-inden-1-yl)picolinamide; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; triphenylborane / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

4: sodium tris(acetoxy)borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5: hydrogenchloride / water; acetonitrile; tert-butyl methyl ether / 40 °C

With hydrogenchloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; triphenylborane; 4-(dimethylamino)-N-((1R,2S)-2-hydroxy-2,3-dihydro-1H-inden-1-yl)picolinamide; sodium tetraphenyl borate; sodium tris(acetoxy)borohydride; sodium hydride; tricyclohexylphosphine; In tetrahydrofuran; dichloromethane; tert-butyl methyl ether; water; acetone; acetonitrile; mineral oil;

Reference yield:

: 122024-75-3,138835-16-2
3-<3-(phenylmethoxy)phenyl>-2-propenoic acid

: 1443156-35-1
(2R,3R)-3-(3-(benzyloxy)phenyl)-N,N,2-trimethylpent-4-en-1-amine hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine; chloroformic acid ethyl ester / 2-methyltetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

1.2: 2 h / 10 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 18 h / 20 - 40 °C / Inert atmosphere

3.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; tricyclohexylphosphine; sodium tetraphenyl borate / dichloromethane; acetone / 14 h / 20 °C / Inert atmosphere

4.1: 4-(dimethylamino)-N-((1R,2S)-2-hydroxy-2,3-dihydro-1H-inden-1-yl)picolinamide; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; triphenylborane / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

5.1: sodium tris(acetoxy)borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride / water; acetonitrile; tert-butyl methyl ether / 40 °C

With hydrogenchloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; triphenylborane; 4-(dimethylamino)-N-((1R,2S)-2-hydroxy-2,3-dihydro-1H-inden-1-yl)picolinamide; sodium tetraphenyl borate; chloroformic acid ethyl ester; sodium tris(acetoxy)borohydride; sodium hydride; triethylamine; tricyclohexylphosphine; In tetrahydrofuran; 2-methyltetrahydrofuran; dichloromethane; tert-butyl methyl ether; water; acetone; acetonitrile; mineral oil;