benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Base Information

Chemical Name:benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate
CAS No.:1448429-83-1
Molecular Formula:C₇₁H₇₈O₁₆
Molecular Weight:1187.39
Hs Code.:

benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Synonyms:benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

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Chemical Property of benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

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Technology Process of benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

There total 1 articles about benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1448429-82-0
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Guidance literature:: With hydrazine hydrate; In pyridine; acetic acid; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201300180

Reference yield: 86.0%

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1603827-04-8
benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyturonate-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-α-n-galactopyranosyl N-phenyltrifluoroacetimidate

: benzyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Guidance literature:: benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate; benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyturonate-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-α-n-galactopyranosyl N-phenyltrifluoroacetimidate; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 0.333333h;

Reference yield: 86.0%

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: C₆₂H₆₀Cl₃F₃N₂O₁₄

: benzyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Guidance literature:: benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate; C₆₂H₆₀Cl₃F₃N₂O₁₄; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 0.333333h;