benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Base Information

Chemical Name:benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate
CAS No.:1448430-02-1
Molecular Formula:C₁₀₀H₁₀₆Cl₃NO₂₁
Molecular Weight:1764.29
Hs Code.:

benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Synonyms:benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

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Chemical Property of benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

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Technology Process of benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

There total 3 articles about benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: N-((2S,3R,4R,5R,6R)-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-(phenylthio)tetrahydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide

: 1448430-02-1
benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Guidance literature:: benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate; N-((2S,3R,4R,5R,6R)-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-2-(phenylthio)tetrahydro-2H-pyran-3-yl)-2,2,2-trichloroacetamide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -60 ℃; for 0.5h;

Reference yield: 80.0%

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: phenyl 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside

: 1448430-02-1
benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1448430-04-3
C₇₄H₈₆O₁₆Si

Guidance literature:: benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate; phenyl 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-1-thio-β-D-galactopyranoside; In dichloromethane; at 20 ℃; for 1h; Microwave irradiation;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In N,N-dimethyl-formamide; at -78 ℃; for 0.5h;
DOI:10.1002/ejoc.201300180

Reference yield: 63.0%

: 1448429-95-5
3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate

: 1448429-83-1
benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1448430-02-1
benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 1448430-03-2
benzyl (3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranosyl)-(1→2)-(4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

Guidance literature:: 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-α/β-D-galactopyranosyl N-phenyltrifluoroacetimidate; benzyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate; In dichloromethane; at 20 ℃; for 1h; Microwave irradiation;

With trimethylsilyl trifluoromethanesulfonate; triethylamine; In N,N-dimethyl-formamide; at -78 ℃; for 0.333333h;
DOI:10.1002/ejoc.201300180