(Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate

Base Information

Chemical Name:(Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate
CAS No.:1533434-97-7
Molecular Formula:C₁₁H₆ClF₃N₄S
Molecular Weight:318.71
Hs Code.:

Synonyms:(Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate

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Technology Process of (Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate

There total 2 articles about (Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1533425-23-8
2-chloro-4-isothiocyanato-6-(trifluoromethyl)benzonitrile

: 19981-17-0,20611-81-8,123092-13-7,17292-62-5
sodium cyanamide

: 74-88-4
methyl iodide

: 1533434-97-7
(Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate

Guidance literature:: 2-chloro-4-isothiocyanato-6-(trifluoromethyl)benzonitrile; sodium cyanamide; In methanol; at 20 ℃; for 1h; under 760.051 Torr; Inert atmosphere;

methyl iodide; In methanol; at 20 ℃; for 18h; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 1095188-09-2
4-amino-2-chloro-6-(trifluoromethyl)benzonitrile

: 1533434-97-7
(Z)-methyl N-(3-chloro-4-cyano-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothiolate

Guidance literature:: Multi-step reaction with 2 steps

1.1: calcium carbonate / dichloromethane; water / 0 - 20 °C / 760.05 Torr / Inert atmosphere

2.1: methanol / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

2.2: 18 h / 20 °C / 760.05 Torr / Inert atmosphere

With calcium carbonate; In methanol; dichloromethane; water;