C₆₅H₁₁₁N₁₃O₉Si₂

Base Information

Chemical Name:C₆₅H₁₁₁N₁₃O₉Si₂
CAS No.:1431217-35-4
Molecular Formula:C₆₅H₁₁₁N₁₃O₉Si₂
Molecular Weight:1274.85
Hs Code.:

C<sub>65</sub>H<sub>111</sub>N<sub>13</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₆₅H₁₁₁N₁₃O₉Si₂

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Chemical Property of C₆₅H₁₁₁N₁₃O₉Si₂

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Technology Process of C₆₅H₁₁₁N₁₃O₉Si₂

There total 17 articles about C₆₅H₁₁₁N₁₃O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1431217-34-3
C₆₄H₁₀₉N₁₃O₉Si₂

: 74-88-4
methyl iodide

: 1431217-35-4
C₆₅H₁₁₁N₁₃O₉Si₂

Guidance literature:: With potassium carbonate; In acetone; for 24h;
DOI:10.1039/c3cc40628h

Reference yield:

: 22818-40-2
D-4-hydroxyphenylglycine

: 1431217-35-4
C₆₅H₁₁₁N₁₃O₉Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: acetic acid; Iodine monochloride / 72 h / 20 °C / Inert atmosphere

2.1: triethylamine / water; 1,4-dioxane

2.2: pH 2 - 3

3.1: sodium hydroxide / dichloromethane; water / 3 h / 0 - 20 °C

3.2: pH 2 - 3

4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

5.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

6.1: trifluoroacetic acid / dichloromethane / 1 h

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

8.1: dimethyl amine; 1-thiopropane / tetrahydrofuran / 1 h

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

10.1: potassium carbonate / acetone / 24 h

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-thiopropane; Iodine monochloride; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dimethyl amine; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetone; 4.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3cc40628h

Reference yield:

: (R)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-6-azidohexanoic acid

: 1431217-35-4
C₆₅H₁₁₁N₁₃O₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

2: trifluoroacetic acid / dichloromethane / 1 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

4: dimethyl amine; 1-thiopropane / tetrahydrofuran / 1 h

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

6: potassium carbonate / acetone / 24 h

With 1-thiopropane; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dimethyl amine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1039/c3cc40628h