PERYLENE-157

Base Information

• Chemical Name: PERYLENE-157
• CAS No.: 156028-28-3
• Molecular Formula: C₇₆H₇₈N₂O₈
• Molecular Weight: 1147.46
• Mol file: 156028-28-3.mol

Synonyms:N,N'-Dicyclohexyl-1,6,7,12-tetrakis(4-tert-butylphenoxy)-3,4:9,10-perylenedicarboximide

Chemical Property of PERYLENE-157

Chemical Property:

• PSA: 115.06000
• LogP: 19.33260

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PERYLENE-157

There total 2 articles about PERYLENE-157 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

para-tert-butylphenol (98-54-4) + N,N’-dicyclohexyl-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid bisimide (156028-27-2) → N,N’-dicyclohexyl-1,6,7,12-tetra(4-tert-butylphenoxy)-perylene-3,4:9,10-tetracarboxylic acid bisimide (156028-28-3)

Guidance literature:

With 1-methyl-pyrrolidin-2-one; potassium carbonate; at 120 ℃; for 20h; Inert atmosphere;

DOI:10.1002/chem.201201484

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) + 1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride (156028-26-1) → N,N’-dicyclohexyl-1,6,7,12-tetra(4-tert-butylphenoxy)-perylene-3,4:9,10-tetracarboxylic acid bisimide (156028-28-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-imidazole / 5 h / 110 °C / Inert atmosphere

2: 1-methyl-pyrrolidin-2-one; potassium carbonate / 20 h / 120 °C / Inert atmosphere

With 1H-imidazole; 1-methyl-pyrrolidin-2-one; potassium carbonate;

DOI:10.1002/chem.201201484

upstream raw materials:

para-tert-butylphenol

N,N’-dicyclohexyl-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid bisimide

cyclohexylamine

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Refernces