(R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

Base Information

Chemical Name:(R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester
CAS No.:133608-98-7
Molecular Formula:C₂₃H₃₄O₆
Molecular Weight:406.519
Hs Code.:

Synonyms:(R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

Suppliers and Price of (R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

There total 2 articles about (R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90315-82-5
ethyl (R)-2-hydroxy-4-phenylbutyrate

: 133608-98-7
(R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / pyridine / CH₂Cl₂ / 0 °C

2: 1) NaH / 1) THF, 1 h, r.t. 2) THF, HMPT, 48 h, r.t.

With pyridine; sodium hydride; In dichloromethane;
DOI:10.1055/s-1991-26405

Reference yield:

: 541-16-2
t-butyl malonate

: 109010-59-5
(R)-2-<(4-nitrobenzolsulfonyl)oxy>-4-phenylbuttersaeure-ethylester

: 133608-98-7
(R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) THF, 1 h, r.t. 2) THF, HMPT, 48 h, r.t.;
DOI:10.1055/s-1991-26405

Reference yield:

: 133608-98-7
(R)-2-tert-Butoxycarbonyl-3-phenethyl-succinic acid 1-tert-butyl ester 4-ethyl ester

: 133609-00-4
(R)-2-Phenethyl-succinic acid 1-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: CF₃CO₂H / 16 h / Ambient temperature

2: Cu₂O / acetonitrile / 6 h / Heating

With copper(I) oxide; trifluoroacetic acid; In acetonitrile;
DOI:10.1055/s-1991-26405