(2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

Base Information

Chemical Name:(2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal
CAS No.:1021394-80-8
Molecular Formula:C₁₇H₁₇NO₃
Molecular Weight:283.327
Hs Code.:

Synonyms:(2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

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Technology Process of (2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

There total 17 articles about (2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 104-53-0
3-phenyl-propionaldehyde

: 5153-67-3
nitrostyrene

: 1021394-80-8
(2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

Guidance literature:: With 4-methyl-morpholine; C₁₆H₂₆N₄O₅; In neat (no solvent); at 20 ℃; for 24h; stereoselective reaction;
DOI:10.1021/acs.joc.0c00665

Reference yield: 99.0%

: 104-53-0
3-phenyl-propionaldehyde

: 5153-67-3
nitrostyrene

: 1089665-81-5
2-benzyl-2-(2-nitro-1-phenylethyl)ethanal

: 1021394-80-8
(2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

: 2-benzyl-4-nitro-3-phenylbutanal

Guidance literature:: With C₁₄H₂₃N₃O₇P^(1-)*BrH*Na⁽¹⁺⁾; In methanol; chloroform; at 0 ℃; for 21h; Reagent/catalyst; Overall yield = > 99 %; stereoselective reaction; Catalytic behavior;
DOI:10.1002/adsc.201500794

Reference yield: 94.0%

: 104-53-0
3-phenyl-propionaldehyde

: 102-96-5
(2-nitroethenyl)benzene

: 1021394-80-8
(2S,3R)-4-nitro-2-(1-phenylmethyl)-3-phenylbutanal

Guidance literature:: With 4-methyl-morpholine; H-D-Pro-L-Pro-L-Glu-NH₂*TFA; In chloroform; isopropyl alcohol; at 20 ℃; optical yield given as %ee;
DOI:10.1002/chem.200901021