1-O--α-D-glucopyranuronic acid

Base Information

Chemical Name:1-O--α-D-glucopyranuronic acid
CAS No.:78008-89-6
Molecular Formula:C₂₀H₂₇NO₁₀
Molecular Weight:441.435
Hs Code.:

1-O-<N-(tert-butoxycarbonyl)-L-phenylalanyl>-α-D-glucopyranuronic acid

Synonyms:1-O--α-D-glucopyranuronic acid

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Chemical Property of 1-O--α-D-glucopyranuronic acid

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Technology Process of 1-O--α-D-glucopyranuronic acid

There total 3 articles about 1-O--α-D-glucopyranuronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 78008-85-2
benzyl 2,3,4-tri-O-benzyl-1-O--D-glucopyranuronate

: 78008-89-6
1-O--α-D-glucopyranuronic acid

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In 2-methoxy-ethanol; for 24h;
DOI:10.1016/S0008-6215(00)84580-2

Reference yield:

: 4539-78-0
2,3,4-tri-O-benzyl-D-glucopyranosideuronic acid benzyl ester

: 78008-89-6
1-O--α-D-glucopyranuronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 185 mg / imidazole / CH₂Cl₂ / 24 h / Ambient temperature

2: 98 percent / H₂, acetic acid / palladium-on-charcoal, 10percent / 2-methoxy-ethanol / 24 h

With 1H-imidazole; hydrogen; acetic acid; palladium on activated charcoal; In dichloromethane; 2-methoxy-ethanol;
DOI:10.1016/S0008-6215(00)84580-2

Reference yield:

: 21148-96-9
N-(tert-butoxycarbonyl)-L-phenylalanine pentachlorophenyl ester

: 78008-89-6
1-O--α-D-glucopyranuronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 185 mg / imidazole / CH₂Cl₂ / 24 h / Ambient temperature

2: 98 percent / H₂, acetic acid / palladium-on-charcoal, 10percent / 2-methoxy-ethanol / 24 h

With 1H-imidazole; hydrogen; acetic acid; palladium on activated charcoal; In dichloromethane; 2-methoxy-ethanol;
DOI:10.1016/S0008-6215(00)84580-2