methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

Base Information

Chemical Name:methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate
CAS No.:1352007-81-8
Molecular Formula:C₂₃H₃₁N₃O₃S
Molecular Weight:429.583
Hs Code.:

Synonyms:methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

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Chemical Property of methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

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Technology Process of methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

There total 5 articles about methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 587887-00-1
1-(2,4,6-trimethylbenzyl)-4,5-dihydroimidazole

: 823785-72-4
(4R,5R)-3,4-dimethyl-5-phenyl-1,2,3-oxathiazolidine-2,2-dioxide

: 1352007-81-8
methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

Guidance literature:: In dichloromethane; at 20 ℃; for 168h;
DOI:10.1016/j.tetasy.2011.09.018

Reference yield:

: C₁₂H₁₈N₂

: 1352007-81-8
methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium tetrahydroborate / 24.33 h / 20 °C / Cooling with ice

2: 2 h / 95 °C / Neat (no solvent)

3: dichloromethane / 168 h / 20 °C

With methanol; sodium tetrahydroborate; In dichloromethane;
DOI:10.1016/j.tetasy.2011.09.018

Reference yield:

: 487-68-3
mesytaldehyde

: 1352007-81-8
methyl((1S,2R)-1-phenyl-1-(1-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)propan-2-yl)sulfamate

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 24 h / 20 °C / Cooling with ice

2: methanol; sodium tetrahydroborate / 24.33 h / 20 °C / Cooling with ice

3: 2 h / 95 °C / Neat (no solvent)

4: dichloromethane / 168 h / 20 °C

With methanol; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2011.09.018