Technology Process of Nickel,[5,9,14,18,23,27,32,36-octabutoxy-37H,39H-tetranaphtho[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazinato(2-)-kN37,kN38,kN39,kN40]-, (SP-4-1)-
There total 1 articles about Nickel,[5,9,14,18,23,27,32,36-octabutoxy-37H,39H-tetranaphtho[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazinato(2-)-kN37,kN38,kN39,kN40]-, (SP-4-1)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
butan-1-ol;
under Ar atm. soln. naphthalocyanine, 1,8-diazabicyclo(5.4.0)undec-7-eneand 1-butanol was treated with Ni(OAc)4*4H2O over 3 days; soln. was diluted with aq. MeOH and filtered, solid was chromd. on alumina (III) (toluene) and vac. dried at room temp.;
DOI:10.1021/ic061524o