N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide

Base Information

Chemical Name:N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide
CAS No.:1152274-52-6
Molecular Formula:C₂₀H₁₇BrN₂O₂
Molecular Weight:397.271
Hs Code.:

Synonyms:N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide

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Chemical Property of N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide

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Technology Process of N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide

There total 1 articles about N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 16728-01-1
1-(4-methoxyphenyl)-1-cyclopropanecarboxylic acid

: 13130-79-5
3-amino-1-bromoisoquinoline

: 1152274-52-6
N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide

Guidance literature:: 1-(4-methoxyphenyl)-1-cyclopropanecarboxylic acid; With thionyl chloride; In N,N-dimethyl-formamide; at 50 ℃; for 4h;

3-amino-1-bromoisoquinoline; With triethylamine; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 1152274-52-6
N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide

: 76-05-1
trifluoroacetic acid

: 1-(4-methoxyphenyl)-N-(1-morpholinoisoquinolin-3-yl)cyclopropanecarboxamide trifluoroacetate

Guidance literature:: morpholine; N-(1-bromoisoquinolin-3-yl)-1-(4-methoxyphenyl)cyclopropanecarboxamide; In 1,4-dioxane; dimethyl sulfoxide; at 170 ℃; for 18h; Microwave;

trifluoroacetic acid; HPLC;