C₃₃H₃₃NO₆

Base Information

Chemical Name:C₃₃H₃₃NO₆
CAS No.:1206725-14-5
Molecular Formula:C₃₃H₃₃NO₆
Molecular Weight:539.628
Hs Code.:

C<sub>33</sub>H<sub>33</sub>NO<sub>6</sub>

Synonyms:C₃₃H₃₃NO₆

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Chemical Property of C₃₃H₃₃NO₆

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Technology Process of C₃₃H₃₃NO₆

There total 2 articles about C₃₃H₃₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 479423-44-4
tert-butyl naphthalen-1-ylmethylenecarbamate

: 15014-25-2
malonic acid dibenzyl ester

: 1206725-14-5
C₃₃H₃₃NO₆

: C₃₃H₃₃NO₆

Guidance literature:: tert-butyl naphthalen-1-ylmethylenecarbamate; With self-assembled organic-inorganic hybrid silica with ionic liquid phase supported ytterbium(III) triflate/isopropyl-pybox 1:2 complex; In dichloromethane; at -18 ℃; for 0.5h; Inert atmosphere;

malonic acid dibenzyl ester; In methanol; dichloromethane; enantioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201402713

Reference yield:

: 479423-31-9
tert-butyl naphthalen-1-yl(phenylsulfonyl)methylcarbamate

: 1206725-14-5
C₃₃H₃₃NO₆

: C₃₃H₃₃NO₆

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; sodium sulfate / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

2: ytterbium(III) triflate; 2,6-bis[(4R)-4,5-dihydro-4-(1-methylethyl)-2-oxazolyl]-pyridine; methanol / dichloromethane / 12 h / 25 °C / Inert atmosphere

With methanol; 2,6-bis[(4R)-4,5-dihydro-4-(1-methylethyl)-2-oxazolyl]-pyridine; potassium carbonate; sodium sulfate; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; 2: |Mannich Aminomethylation;
DOI:10.1002/chem.201300241