C₅₁H₆₃N₃O₁₂S₃

Base Information

• Chemical Name: C₅₁H₆₃N₃O₁₂S₃
• CAS No.: 213555-21-6
• Molecular Formula: C₅₁H₆₃N₃O₁₂S₃
• Molecular Weight: 1006.27
• Mol file: 213555-21-6.mol

Synonyms:C₅₁H₆₃N₃O₁₂S₃

Chemical Property of C₅₁H₆₃N₃O₁₂S₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₅₁H₆₃N₃O₁₂S₃

There total 4 articles about C₅₁H₆₃N₃O₁₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

1,3,5-tris[4'-(tosyloxy)-2'-oxa-1'-butyl]benzene (152065-65-1) + 1,3,5-tris[5'(p-toluenesulfonyl)-2'-oxa-5'-azapentyl]benzene (213555-14-7) → C51H63N3O12S3 (213555-21-6)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 75 - 80 ℃; for 48h;

DOI:10.1002/jhet.5570350305

Reference yield:

N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide (18303-04-3) → C51H63N3O12S3 (213555-21-6)

Guidance literature:

Multi-step reaction with 3 steps

1: Ph₃P, diethylazodicarboxylate / tetrahydrofuran / 18 h

2: aq. HCl / propan-2-ol; CH₂Cl₂ / 48 h

3: 41 percent / Cs₂CO₃ / dimethylformamide / 48 h / 75 - 80 °C

With hydrogenchloride; caesium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

DOI:10.1002/jhet.5570350305

Reference yield:

1,3,5-tris-((2'-hydroxy)ethoxymethyl)benzene (152065-61-7) → C51H63N3O12S3 (213555-21-6)

Guidance literature:

Multi-step reaction with 3 steps

1: Ph₃P, diethylazodicarboxylate / tetrahydrofuran / 18 h

2: aq. HCl / propan-2-ol; CH₂Cl₂ / 48 h

3: 41 percent / Cs₂CO₃ / dimethylformamide / 48 h / 75 - 80 °C

With hydrogenchloride; caesium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

DOI:10.1002/jhet.5570350305

upstream raw materials:

1,3,5-tris[4'-(tosyloxy)-2'-oxa-1'-butyl]benzene

1,3,5-tris[5'(p-toluenesulfonyl)-2'-oxa-5'-azapentyl]benzene

N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

1,3,5-tris-((2'-hydroxy)ethoxymethyl)benzene