(S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Base Information

Chemical Name:(S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester
CAS No.:129679-79-4
Molecular Formula:C₂₅H₄₂N₂O₅S₂Si
Molecular Weight:542.836
Hs Code.:

Synonyms:(S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Suppliers and Price of (S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

There total 4 articles about (S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 129679-79-4
(S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) BF₃*Et₂O, 2.) aq. NaHCO₃ / 1.) CH₂Cl₂, 23 deg C, 2.) 23 deg C

3: 80 percent / Zn, AcOH / diethyl ether / 23 °C

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; acetic acid; zinc; In diethyl ether;
DOI:10.1021/ja00175a043

Reference yield:

: 129679-78-3
(S)-2-tert-Butoxycarbonylamino-pentane-bis-thioic acid di-S-ethyl ester

: 129679-79-4
(S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BF₃*Et₂O, 2.) aq. NaHCO₃ / 1.) CH₂Cl₂, 23 deg C, 2.) 23 deg C

2: 80 percent / Zn, AcOH / diethyl ether / 23 °C

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; acetic acid; zinc; In diethyl ether;
DOI:10.1021/ja00175a043

Reference yield:

: 129679-77-2
4-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-2-nitro-benzoyl chloride

: 129679-79-4
(S)-2-{2-Amino-4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-5-methoxy-benzoylamino}-pentane-bis-thioic acid di-S-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BF₃*Et₂O, 2.) aq. NaHCO₃ / 1.) CH₂Cl₂, 23 deg C, 2.) 23 deg C

2: 80 percent / Zn, AcOH / diethyl ether / 23 °C

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; acetic acid; zinc; In diethyl ether;
DOI:10.1021/ja00175a043