bis(3,5-difluorophenyl)diphenyl stannane

Base Information

Chemical Name:bis(3,5-difluorophenyl)diphenyl stannane
CAS No.:1054621-26-9
Molecular Formula:C₂₄H₁₆F₄Sn
Molecular Weight:499.095
Hs Code.:

Synonyms:bis(3,5-difluorophenyl)diphenyl stannane

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Chemical Property of bis(3,5-difluorophenyl)diphenyl stannane

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Technology Process of bis(3,5-difluorophenyl)diphenyl stannane

There total 1 articles about bis(3,5-difluorophenyl)diphenyl stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 461-96-1
3,5-difluorobromobenzene

: 1135-99-5
diphenyltin(IV) dichloride

: 1054621-26-9
bis(3,5-difluorophenyl)diphenyl stannane

Guidance literature:: With Mg; I₂; In diethyl ether; (N2); addn. of iodine and ethereal soln. of bromide deriv. to magnesium,keeping for 15 min, addn. of addnl. soln. of bromide deriv. in ether, r efluxing for 1 h, cooling to room temp., addn. of soln. of tin compd. inether, refluxing for 2 h; addn. of aq. HCl, extn. (diethyl ether), drying over MgSO4, filtration, evapn., recrystn. (ethanol), elem. anal.;
DOI:10.1021/ic800664f

Reference yield: 69.0%

: 1054621-26-9
bis(3,5-difluorophenyl)diphenyl stannane

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 1054621-20-3
bis(3,5-bis(diphenylphosphino)phenyl)diphenyl stannane

Guidance literature:: In tetrahydrofuran; (N2); addn. of THF soln. of phosphide deriv. to tin compd., stirring at room temp. for 1 h, refluxing overnight; elem. anal.;
DOI:10.1021/ic800664f