W=N(C₆H₅)(CH₂CMe₃)3Cl

Base Information

Chemical Name:W=N(C₆H₅)(CH₂CMe₃)3Cl
CAS No.:83634-51-9
Molecular Formula:C₂₁H₃₈ClNW
Molecular Weight:523.842
Hs Code.:

W=N(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>CMe<sub>3</sub>)3Cl

Synonyms:W=N(C₆H₅)(CH₂CMe₃)3Cl

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Chemical Property of W=N(C₆H₅)(CH₂CMe₃)3Cl

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Technology Process of W=N(C₆H₅)(CH₂CMe₃)3Cl

There total 4 articles about W=N(C₆H₅)(CH₂CMe₃)3Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: Cl₄(OEt₂)W(NPh)

: 13132-23-5
2,2-dimethylpropylmagnesium chloride

: 83634-51-9
W(NC₆H₅)(CH₂C(CH₃)3)3Cl

Guidance literature:: In diethyl ether; Mg compd. added to ether soln. of W complex at -78°C under N2, mixture warmed to room temp., kept at this temp. for 24 h; filtration through Celite, washing with Et2O, removal of solvent in vac., dissolving in pentane, treatment with activated charcoal, filtration,evapn. in vac., sublimation at 80-90°C (0.001 mm Hg); elem. anal.;
DOI:10.1021/ja00390a016