N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide
CAS No.:927807-99-6
Molecular Formula:C₂₃H₂₉NO₄S
Molecular Weight:415.554
Hs Code.:

Synonyms:N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

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Technology Process of N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

There total 3 articles about N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 919116-90-8
N-allyl-N-(1-benzyloxymethyl-3-oxopropyl)-4-methylbenzenesulfonamide

: 1826-67-1
vinyl magnesium bromide

: 927808-00-2
N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

: 927807-99-6
N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

Guidance literature:: In tetrahydrofuran; toluene; at -78 ℃; for 2h;
DOI:10.1016/j.tet.2006.12.002

Reference yield:

: 919116-85-1
(2S)-N-allyl-N-[1-benzyloxymethyl-3-(t-butyldimethylsilanyloxy)propyl]-4-methylbenzenesulfonamide

: 927807-99-6
N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-n-butyl-ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

1.2: 84 percent / pyridinium chlorochromate; Celite / tetrahydrofuran; CH₂Cl₂ / 10 h / 20 °C

2.1: 47 percent / tetrahydrofuran; toluene / 2 h / -78 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; toluene; 2.1: Grignard addition;
DOI:10.1016/j.tet.2006.12.002

Reference yield:

: 115344-32-6
(2S)-N-(1-benzyloxymethyl-3-hydroxypropyl)-4-methylbenzenesulfonamide

: 927807-99-6
N-allyl-N-(1-benzyloxymethyl-3-hydroxypent-4-enyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethylformamide / 10 h / 20 °C

1.2: 80 percent / dimethylformamide / 5 h / 20 °C

2.1: tetra-n-butyl-ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2.2: 84 percent / pyridinium chlorochromate; Celite / tetrahydrofuran; CH₂Cl₂ / 10 h / 20 °C

3.1: 47 percent / tetrahydrofuran; toluene / 2 h / -78 °C

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 3.1: Grignard addition;
DOI:10.1016/j.tet.2006.12.002