C₆₀H₁₂F₃₀

Base Information

• Chemical Name: C₆₀H₁₂F₃₀
• CAS No.: 262422-64-0
• Molecular Formula: C₆₀H₁₂F₃₀
• Molecular Weight: 1302.71
• Mol file: 262422-64-0.mol

Synonyms:C₆₀H₁₂F₃₀

Chemical Property of C₆₀H₁₂F₃₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₁₂F₃₀

There total 4 articles about C₆₀H₁₂F₃₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

2,4,6-trifluorobromobenzene (2367-76-2) + C24Br6F12 (262422-60-6) → C60H12F30 (262422-64-0)

Guidance literature:

2,4,6-trifluorobromobenzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 24h;

With copper(I) bromide; In tetrahydrofuran; at 20 ℃; for 1h;

C₂₄Br₆F₁₂; In tetrahydrofuran; 1,4-dioxane; toluene; for 4h; Further stages.; Heating;

DOI:10.1021/ja994083z

Reference yield:

1,3,5-tribromo-2,4,6-trifluoro-benzene (2368-49-2) → C60H12F30 (262422-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: Mg / tetrahydrofuran / 1 h / 20 °C

1.2: CuBr / tetrahydrofuran / 1 h / 20 °C

1.3: 69 percent / tetrahydrofuran; toluene; dioxane / 96 h / 80 °C

2.1: 79 percent / Fe; Br₂ / 72 h / Heating

3.1: Mg / tetrahydrofuran / 24 h / 20 °C

3.2: CuBr / tetrahydrofuran / 1 h / 20 °C

3.3: 44 percent / tetrahydrofuran; toluene; dioxane / 4 h / Heating

With bromine; iron; magnesium; In tetrahydrofuran; 1.1: Metallation / 1.2: Substitution / 1.3: cross-coupling reaction / 2.1: Bromination / 3.1: Metallation / 3.2: Substitution / 3.3: cross-coupling reaction;

DOI:10.1021/ja994083z

Reference yield:

2,4,6-trifluorobromobenzene (2367-76-2) → C60H12F30 (262422-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: Mg / tetrahydrofuran / 1 h / 20 °C

1.2: CuBr / tetrahydrofuran / 1 h / 20 °C

1.3: 69 percent / tetrahydrofuran; toluene; dioxane / 96 h / 80 °C

2.1: 79 percent / Fe; Br₂ / 72 h / Heating

3.1: Mg / tetrahydrofuran / 24 h / 20 °C

3.2: CuBr / tetrahydrofuran / 1 h / 20 °C

3.3: 44 percent / tetrahydrofuran; toluene; dioxane / 4 h / Heating

With bromine; iron; magnesium; In tetrahydrofuran; 1.1: Metallation / 1.2: Substitution / 1.3: cross-coupling reaction / 2.1: Bromination / 3.1: Metallation / 3.2: Substitution / 3.3: cross-coupling reaction;

DOI:10.1021/ja994083z

upstream raw materials:

2,4,6-trifluorobromobenzene

C₂₄Br₆F₁₂

1,3,5-tribromo-2,4,6-trifluoro-benzene

C₂₄H₆F₁₂

Downstream raw materials:

C₆₀Br₁₂F₃₀