[({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

Base Information

• Chemical Name: [({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester
• CAS No.: 76337-88-7
• Molecular Formula: C₂₅H₂₁ClN₄O₇
• Molecular Weight: 524.917

Synonyms:[({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

Chemical Property of [({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

Chemical Property:

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Technology Process of [({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

There total 2 articles about [({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester (76337-80-9) → [({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester (76337-88-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 30percent HBr / acetic acid / 1.5 h / Ambient temperature

2: hexamethylphosphoric acid triamide / Ambient temperature

With hydrogen bromide; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid;

DOI:10.1021/jm00133a006

Reference yield:

N-(benzyloxycarbonyl)glycyl chloride (15050-24-5) + 2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-acetamide; hydrobromide (76337-85-4) → [({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester (76337-88-7)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; Yield given; Ambient temperature;

DOI:10.1021/jm00133a006

Reference yield: 89.0%

[({[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester (76337-88-7) → 2-Amino-N-{[2-(2-chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-acetamide; hydrobromide (76337-90-1)

Guidance literature:

With hydrogen bromide; In acetic acid; for 1h; Ambient temperature;

DOI:10.1021/jm00133a006

upstream raw materials:

N-(benzyloxycarbonyl)glycyl chloride

2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-acetamide; hydrobromide

{[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

Downstream raw materials:

2-Amino-N-{[2-(2-chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-acetamide; hydrobromide

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