5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside
CAS No.:866934-18-1
Molecular Formula:C₃₈H₃₃NO₉S₂
Molecular Weight:711.813
Hs Code.:

Synonyms:5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

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Chemical Property of 5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

There total 5 articles about 5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 5554-48-3
Tetrahydro-1,3-thiazin-2-thion

: 866934-18-1
5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: 14125-75-8
2,3,4,6-tetra-O-benzoyl-D-hydroxyglucal

Guidance literature:: With potassium hydroxide; 18-crown-6 ether; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1080/07328300500176387

Reference yield:

: 866934-17-0
5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

: 866934-18-1
5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methoxide / methanol / 3 h / 20 °C / pH 9

2: pyridine / 16 h / 20 °C

With pyridine; sodium methylate; In methanol;
DOI:10.1080/07328300500176387

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 866934-18-1
5,6-dihydro-4H-1,3-thiazin-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 22 percent / potassium hydroxide / acetonitrile / 1 h / 20 °C

2: sodium methoxide / methanol / 3 h / 20 °C / pH 9

3: pyridine / 16 h / 20 °C

With pyridine; potassium hydroxide; sodium methylate; In methanol; acetonitrile;
DOI:10.1080/07328300500176387