(2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

Base Information

Chemical Name:(2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine
CAS No.:207598-56-9
Molecular Formula:C₁₇H₂₃N₂O₇P
Molecular Weight:398.353
Hs Code.:

Synonyms:(2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

There total 2 articles about (2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: (2R,4aR,5aR,8aR,8bS)-2-Chloro-3-isopropyl-7,7-dimethyl-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

: 207598-56-9
(2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

Guidance literature:: With triethylamine; In chloroform; at 50 ℃;
DOI:10.1021/jo972318o

Reference yield:

: 187342-10-5
5-deoxy-5-isopropylamino-1,2-O-isopropylidene-α-D-xylofuranose

: 207598-56-9
(2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₃, Et₃N / CHCl₃ / 50 °C

2: 78 percent / Et₃N / CHCl₃ / 50 °C

With triethylamine; phosphorus trichloride; In chloroform;
DOI:10.1021/jo972318o

Reference yield:

: 207598-56-9
(2R,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine

: (2S,4aR,5aR,8aR,8bS)-3-Isopropyl-7,7-dimethyl-2-(4-nitro-phenoxy)-hexahydro-[1,3]dioxolo[4,5]furo[2,3-e][1,3,2]oxazaphosphinine 2-sulfide

Guidance literature:: With 3H-1,2-Benzodithiol-3-one 1,1-dioxide; In dichloromethane; for 0.0833333h; Yield given; Ambient temperature;
DOI:10.1021/jo972318o