(E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

Base Information

Chemical Name:(E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester
CAS No.:1059574-69-4
Molecular Formula:C₄₀H₄₁O₃PSi
Molecular Weight:628.823
Hs Code.:

Synonyms:(E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

Suppliers and Price of (E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

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Technology Process of (E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

There total 1 articles about (E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 17261-28-8
ortho-diphenylphosphinobenzoic acid

: 182006-63-9
(E)-1-(tert-butyldiphenylsilyloxy)pent-3-en-2-ol

: 1059574-69-4
(E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1055/s-2008-1067140

Reference yield:

: 1059574-69-4
(E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester

: 201230-82-2
carbon monoxide

: C₄₁H₄₃O₄PSi

Guidance literature:: (E)-o-diphenylphosphanylbenzoic acid 1-(tert-butyldiphenylsilyloxymethyl)but-2-enyl ester; With (acetylacetonato)dicarbonylrhodium (l); In tetrahydrofuran; for 0.0833333h; Autoclave; Inert atmosphere;

carbon monoxide; With hydrogen; In tetrahydrofuran; at 50 ℃; for 48h; under 30003 Torr; regioselective reaction; Autoclave;
DOI:10.1055/s-2008-1067140