4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol

Base Information

• Chemical Name: 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol
• CAS No.: 1259518-15-4
• Molecular Formula: C₁₈H₁₇ClN₂O₃
• Molecular Weight: 344.798

Synonyms:4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol

Chemical Property of 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol

Chemical Property:

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Technology Process of 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol

There total 1 articles about 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-3-{2-methyl-4-[({[2-(trimethylsilyl)ethyl]oxy}methyl)oxy]phenyl}-1,2,4-oxadiazole (1259517-50-4) → 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol (1259518-15-4)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrabutyl ammonium fluoride; at 20 - 40 ℃; for 27h;

Reference yield:

ethyl 5-bromovalerate (14660-52-7) + 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol (1259518-15-4) → ethyl 5-{[4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenyl]oxy}pentanoate (1259517-52-6)

Guidance literature:

With potassium carbonate; In acetone; at 60 ℃;

Reference yield:

Ethyl 4-bromobutyrate (2969-81-5) + 4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenol (1259518-15-4) → ethyl 4-{[4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenyl]oxy}butanoate (1259517-51-5)

Guidance literature:

With potassium carbonate; In acetone; at 60 ℃;

upstream raw materials:

5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-3-{2-methyl-4-[({[2-(trimethylsilyl)ethyl]oxy}methyl)oxy]phenyl}-1,2,4-oxadiazole

Downstream raw materials:

ethyl 5-{[4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenyl]oxy}pentanoate

ethyl 4-{[4-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-3-methylphenyl]oxy}butanoate

3-(4-[(3-bromopropyl)oxy]-2-methylphenyl)-5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazole

3-{4-[(2-bromoethyl)oxy]-2-methylphenyl}-5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-l,2,4-oxadiazole

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