1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

Base Information

Chemical Name:1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate
CAS No.:1453114-90-3
Molecular Formula:BF₄*C₂₅H₄₀N₃
Molecular Weight:469.417
Hs Code.:

Synonyms:1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

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Chemical Property of 1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

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Technology Process of 1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

There total 10 articles about 1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13755-29-8
sodium tetrafluoroborate

: C₂₅H₄₀N₃⁽¹⁺⁾*Br^(1-)

: 1453114-90-3
1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

Guidance literature:: In acetone; at 20 ℃;
DOI:10.1016/j.tetasy.2013.07.013

Reference yield:

: 31795-93-4
N-benzyl-L-proline

: 1453114-90-3
1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 8.17 h / Reflux

3.1: hydrazine / ethanol / 2 h / Reflux

3.2: 0.5 h / Heating

4.1: methanol / 20 °C

5.1: ethanol / 3 h / Reflux

6.1: nickel / ethanol / 20 °C

7.1: acetonitrile / 16 h / Reflux

8.1: acetone / 20 °C

With lithium aluminium tetrahydride; nickel; triphenylphosphine; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; acetone; acetonitrile;
DOI:10.1016/j.tetasy.2013.07.013

Reference yield:

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 1453114-90-3
1-{[(2S)-N-benzylpyrrolidin-2-yl]methyl}-4,5-dimethyl-3-octyl-1H-imidazolium tetrafluoroborate

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium hydroxide / isopropyl alcohol

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 8.17 h / Reflux

4.1: hydrazine / ethanol / 2 h / Reflux

4.2: 0.5 h / Heating

5.1: methanol / 20 °C

6.1: ethanol / 3 h / Reflux

7.1: nickel / ethanol / 20 °C

8.1: acetonitrile / 16 h / Reflux

9.1: acetone / 20 °C

With lithium aluminium tetrahydride; nickel; triphenylphosphine; potassium hydroxide; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; isopropyl alcohol; acetone; acetonitrile;
DOI:10.1016/j.tetasy.2013.07.013