Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

Base Information

Chemical Name:Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate
CAS No.:1202576-79-1
Molecular Formula:C₂₂H₂₉NO₆S
Molecular Weight:435.541
Hs Code.:

Synonyms:Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

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Chemical Property of Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

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Technology Process of Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

There total 6 articles about Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 137638-70-1
3-(bromomethyl)-N,N-dimethylbenzenesulfonamide

: 1202576-67-7
ethyl 3-ethoxy-3-(4-hydroxyphenyl)propionate

: 1202576-79-1
Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

Guidance literature:: With potassium carbonate; In acetone; at 20 - 60 ℃; Inert atmosphere;

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 1202576-79-1
Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

2: silver(l) oxide / toluene / 20 - 100 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4: potassium carbonate / acetone / 20 - 60 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; potassium carbonate; silver(l) oxide; In tetrahydrofuran; acetone; toluene;

Reference yield:

: 1899-93-0
3-methylphenylsulfonyl chloride

: 1202576-79-1
Ethyl 3-[4-({3-[(dimethylamino)sulfonyl]benzyl}oxy)phenyl]-3-ethoxypropionate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / tetrahydrofuran / 0 - 20 °C

2: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 3 h / Reflux

3: potassium carbonate / acetone / 20 - 60 °C / Inert atmosphere

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrahydrofuran; tetrachloromethane; acetone;