C₅₁H₆₈N₄O₁₂

Base Information

Chemical Name:C₅₁H₆₈N₄O₁₂
CAS No.:1419389-00-6
Molecular Formula:C₅₁H₆₈N₄O₁₂
Molecular Weight:929.121
Hs Code.:

C<sub>51</sub>H<sub>68</sub>N<sub>4</sub>O<sub>12</sub>

Synonyms:C₅₁H₆₈N₄O₁₂

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Chemical Property of C₅₁H₆₈N₄O₁₂

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Technology Process of C₅₁H₆₈N₄O₁₂

There total 11 articles about C₅₁H₆₈N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.8%

: 1296797-05-1
C₁₄H₂₄N₂O₅

: 1419387-69-1
C₂₃H₂₂Br₂O₂

: 1419389-00-6
C₅₁H₆₈N₄O₁₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 - 20 ℃;

Reference yield:

: 1419386-48-3
C₁₄H₁₆O₂

: 1419389-00-6
C₅₁H₆₈N₄O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

3.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

4.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C / Inert atmosphere

6.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

6.2: 4 h / 0 °C

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0 - 20 °C

With pyridine; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 13336-31-7
4-methoxylindanone

: 1419389-00-6
C₅₁H₆₈N₄O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium tert-butylate / toluene / 3.5 h / 80 °C / Inert atmosphere; Cooling with ice

2.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

3.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

4.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C / Inert atmosphere

7.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

7.2: 4 h / 0 °C

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0 - 20 °C

With pyridine; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; potassium tert-butylate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; toluene; acetonitrile;