bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

Base Information

Chemical Name:bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)
CAS No.:88363-91-1
Molecular Formula:C₂₄H₂₀Fe₄O₂S₆*2C₂₄H₂₀P
Molecular Weight:1435
Hs Code.:

Synonyms:bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

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Chemical Property of bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

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Technology Process of bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

There total 2 articles about bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 80939-30-6
bis(tetraphenylphosphonium) bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

: 100-67-4
potassium phenolate

: 88363-91-1
bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

Guidance literature:: In ethanol; acetonitrile; to MeCN soln. of Fe complex was added ethanolic soln. of KOPh dropwise with stirring over 10 min; filtration, adding of Et2O, standing overnight, isolation, drying in vac.; elem anal.;
DOI:10.1021/ja00328a033

Reference yield:

: 84032-42-8
2P(C₆H₅)4⁽¹⁺⁾*{Fe₂S₂(SC₆H₅)4}^(2-) = {P(C₆H₅)4}2{Fe₂S₂(SC₆H₅)4}

: 88363-91-1
bis(tetraphenylphosphonium) bis(phenolato)bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide

2: acetonitrile; ethanol

In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00328a033