ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate

Base Information

• Chemical Name: ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate
• CAS No.: 699016-65-4
• Molecular Formula: C₃₅H₄₁ClN₂O₁₀S
• Molecular Weight: 717.237

Synonyms:ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate

Chemical Property of ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate

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Technology Process of ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate

There total 1 articles about ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) + ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate (699015-63-9) → ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate (699016-65-4)

Guidance literature:

pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]amino]ethyl]phenyl]-sulfonyl]-2-nitrobenzoate (699016-65-4) → ethyl 2-amino-5-[[4-[2-[(tert-butoxycarbonyl)-[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)-ethyl]amino]ethyl]phenyl]sulfonyl]benzoate (699016-66-5)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; for 0.5h; Heating / reflux;

upstream raw materials:

3,4-dihydro-2H-pyran

ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

Downstream raw materials:

ethyl 2-amino-5-[[4-[2-[(tert-butoxycarbonyl)-[(2R)-2-(3-chlorophenyl)-2-(tetrahydro-2H-pyran-2-yloxy)-ethyl]amino]ethyl]phenyl]sulfonyl]benzoate

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